HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylimidazole → HCID 69557324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylimidazole | HCID 69591 | — |
| Reactant | 4-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]butyl methanesulfonate | HCID 15521676 | — |
| Product | HCID 69557324 | HCID 69557324 | 40% |
Reaction Steps
In substantially the same manner as in Working Example 8, 2-phenylimidazole was allowed to react with 4-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]butyl methanesulfonate to give 2-[(E)-2-phenylethenyl]-4-[4-[4-(2-phenyl-1-imidazolyl) butyl]phenoxymethyl]oxazole. The yield was 40%. Recrystallization from ethyl acetate-isopropyl ether gave colorless prisms, mp 85-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-2b3aedb965ba4f6a9011ccc8c4e7a734 |
| Source note | uspto-grants-2001_04 |