4,5-Diphenylimidazole → HCID 22009650, Verbindung

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	4,5-Diphenylimidazole	HCID 69588	—
Edukt	3-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propyl methanesulfonate	HCID 15521674	—
Produkt	HCID 22009650	HCID 22009650	53%

Reaktionsschritte

In substantially the same manner as in Working Example 25, 3-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propyl methanesulfonate was allowed to react with 4,5-diphenylimidazole to give 4-[4-[3-(4,5-diphenyl-1-imidazolyl)propyl]phenoxymethyl]-2-[(E)-2-phenylethenyl]oxazole. The yield was 53%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 137-138° C.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06211215B1
Quelldatensatz	uspto-grants-2001_04
ORD ID	ord-cc6b7c4992ea4fd9956d53d48e82b2d4
Quellennotiz	uspto-grants-2001_04