HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[3-(4-Hydroxyphenyl)propyl]imidazole → HCID 22009626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[3-(4-Hydroxyphenyl)propyl]imidazole | HCID 22009818 | — |
| Reactant | HCID 22009858 | HCID 22009858 | — |
| Product | HCID 22009626 | HCID 22009626 | 68% |
Reaction Steps
In substantially the same manner as in Working Example 48, 1-[3-(4-hydroxyphenyl)propyl]imidazole was allowed to react with 2-(2-benzo[b]thienyl)-4-chloromethyloxazole to give 2-(2-benzo[b]thienyl)-4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole. The yield was 68%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 149-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-03997a533e7f4fd4abdcdd6f11e5883c |
| Source note | uspto-grants-2001_04 |