HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → HCID 22009769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | HCID 135819169 | HCID 135819169 | — |
| Product | HCID 22009769 | HCID 22009769 | 30% |
Reaction Steps
In substantially the same manner as in Working Example 131, 2-(4-hydroxyphenyl)-4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole was allowed to react with 4-chlorobenzylchloride to give 2-[4-(4-chlorobenzyloxy)phenyl]-4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole. The yield was 30%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 151-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-cadd765ec2704a94998305fd44845dd5 |
| Source note | uspto-grants-2001_04 |