HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 22009774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 22009837 | HCID 22009837 | — |
| Product | HCID 22009774 | HCID 22009774 | 92% |
Reaction Steps
In substantially the same manner as in Working Example 135, 2-(5-bromo-2-furyl)-4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole was allowed to react with phenylboronic acid to give 4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]-2-(5-phenyl-2-furyl)oxazole. The yield was 92%. Recrystallization from ethyl acetate-isopropyl ether gave colorless needles, mp 130-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-3ff084965a1940d5b7ad5c5e88fbbe0e |
| Source note | uspto-grants-2001_04 |