HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[4-(4-Hydroxyphenyl)butyl]imidazole → HCID 22009724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[4-(4-Hydroxyphenyl)butyl]imidazole | HCID 22009664 | — |
| Reactant | HCID 22009850 | HCID 22009850 | — |
| Product | HCID 22009724 | HCID 22009724 | 74% |
Reaction Steps
In substantially the same manner as in Working Example 72, 1-[4-(4-hydroxyphenyl)butyl]imidazole was reacted with 4-chloromethyl-2-(5-methyl-2-thienyl)thiazole to obtain 4-[4-[4-(1-imidazolyl)butyl]phenoxymethyl]-2-(5-methyl-2-thienyl)thiazole. The yield was 74%. Recrystallization from ethyl acetate-hexane gave pale yellow needles, mp 81-82° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f556424e7bf44ff98344aa7b4f1f3e27 |
| Source note | uspto-grants-2001_04 |