HCID 53887243, compound → HCID 54206464, compound

HRID 322514Notes

Reaction equation

HRID 322514 reaction equation
C([CH:3]([C@H:7]([NH:14][C:15](=[O:35])[CH2:16][N:17]1[CH2:21][CH2:20][C@H:19]([NH:22][CH2:23][C:24]2[CH:33]=[CH:32][C:31]3[CH2:30][CH2:29][CH2:28][NH:27][C:26]=3[N:25]=2)[C:18]1=[O:34])[C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[C:4]([OH:6])=[O:5])C>Cl>[O:34]=[C:18]1[C@@H:19]([NH:22][CH2:23][C:24]2[CH:33]=[CH:32][C:31]3[CH2:30][CH2:29][CH2:28][NH:27][C:26]=3[N:25]=2)[CH2:20][CH2:21][N:17]1[CH2:16][C:15]([NH:14][C@H:7]([C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)[CH2:3][C:4]([OH:6])=[O:5])=[O:35]

Participants

3

Reactant 1

HCID 53887243HCID 53887243, compound

Product 1

HCID 54206464HCID 54206464, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

9-8 (25 mg, 0.043 mmol) was dissolved in 6N HCl (2 mL) and stirred at room temperature for 16 h, then evaporated to afford 9-9 as a pale yellow solid.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-e1c3e341064a415896cd0ffcc90af9ab
Source dataset
uspto-grants-2001_04
Patent number
US06211184B1

Reaction notes

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