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HRID322722

反应详情

EQUATION

反应方程式

HRID 322722 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)[C@@H](N)CCCCNC(=O)OC(C)(C)C
HCID7018776

未命名化合物

结构：C[C@H](NC(=O)Cc1cc(F)cc(F)c1)C(=O)O
HCID12135350

N-[(3,5-difluorophenyl)acetyl]alanine

C11H11F2NO3

PRODUCTS

生成物

1
结构：COC(=O)[C@H](CCCCNC(=O)OC(C)(C)C)NC(=O)[C@H](C)NC(=O)Cc1cc(F)cc(F)c1
HCID20642604

未命名化合物

PROCEDURE

实验过程

Following General Procedure A and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2 above) and Nε-(tert-butoxycarbonyl)-L-lysine methyl ester (Bachem), the title compound was prepared as an oil. The reaction was monitored by tlc (Rf=0.40 in 50% EtOAc/hexanes) and the product was purified by flash chromotography using 50% EtOAc/hexanes as the eluent.

WORKUP

后处理

  1. customthe product was purified by flash chromotography