HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 131722477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 131722478 | HCID 131722478 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 131722477 | HCID 131722477 | — |
Reaction Steps
A solution of 364 mg of t-butoxycarbonyl phenylglycine thiocarboxamide in 4 mL 30% HBr in acetic acid was stirred for 1 hour. The volitile materials were removed under reduced pressure and the crude phenylglycine thiocarboxamide hydrobromide was obtained as a pale solid. The material was utilized without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211235B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-567bca1b16cc4c98ba92fd3ac8e3d3a5 |
| Source note | uspto-grants-2001_04 |