反应详情

A stirred suspension of 3-iodobenzoic acid (8.84 g) in thionyl chloride (44 mL) is heated at reflux for 30 minutes. The dark brown solution is evaporated to give 3-iodobenzoyl chloride (9.8 g) as a brown oil.

1. temperatureis heated
2. temperatureat reflux for 30 minutes
3. customThe dark brown solution is evaporated