HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodobenzoic acid → 3-Iodobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodobenzoic acid | HCID 12060 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 3-Iodobenzoyl chloride | HCID 74378 | — |
Reaction Steps
A stirred suspension of 3-iodobenzoic acid (8.84 g) in thionyl chloride (44 mL) is heated at reflux for 30 minutes. The dark brown solution is evaporated to give 3-iodobenzoyl chloride (9.8 g) as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211234B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-b827ff56829d41e09cc67ff193ea896a |
| Source note | uspto-grants-2001_04 |