HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → HCID 70228322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | Ethyl 3-amino-5-(trimethylsilyl)-4-pentynoate | HCID 10353172 | — |
| Product | HCID 70228322 | HCID 70228322 | — |
Reaction Steps
Preparation phenyl acetic acid salt of racemic ethyl 3-amino-5-(trimethylsilyl)-4-pentynoate. Racemic ethyl 3-amino-5-(trimethylsilyl)-4-pentynoate (67 g) was reacted with 39 g of phenylacetic acid. The product was filtered and washed with hexane and dried in a vacuum oven to give 100 g the desired racemic ethyl 3-amino-5-(trimethylsilyl)-4-pentynoate phenyl acetic acid salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214609B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-a5cb53db7c87452a8cbc676fa3a14df8 |
| Source note | uspto-grants-2001_04 |