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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 323772Generated: October 29, 2026

Triethylamine → HCID 9838011, compound

https://huagongshe.com/reaction/323772

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantCyclopropanecarbonyl chlorideHCID 77637—
ReactantHCID 54474819HCID 54474819—
ProductHCID 9838011HCID 983801143.3%

Reaction Steps

The title compound was prepared by the general procedure described in Example 1 using (cis)-2-(2,3-dihydrobenzofuran-4-yl)cycloprop-1-yl methyl amine (0.79 mmol), triethylamine (2.37 mmol) and cyclopropane carbonyl chloride (0.95 mmol). Purification by silica gel column chromatography (Hex:EtOAc, 2:1) provided 88 mg of the desired product (43%) as a white wax. HPLC purity=92%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06214869B1
Source datasetuspto-grants-2001_04
ORD IDord-d348a591e1cc4b59ae47a209ce7006b2
Source noteuspto-grants-2001_04