HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9795147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Reactant | HCID 54474819 | HCID 54474819 | — |
| Product | HCID 9795147 | HCID 9795147 | 37.1% |
Reaction Steps
The title compound was prepared by the general procedure described in Example 1 using (cis)-2-(2,3-dihydrobenzofuran-4-yl)cycloprop-1-yl methyl amine (0.79 mmol), triethylamine (2.37 mmol) and isobutyryl chloride (0.95 mmol). Purification by recrystallization from EtOAc/Hexanes provided 76 mg of the desired product (37%) as colorless plates. HPLC purity>98%. m.p. 125-126°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214869B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-3aa123863fc3470496e7525d60f4347e |
| Source note | uspto-grants-2001_04 |