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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 323786Generated: October 29, 2026

HCID 22007146, compound → HCID 22007147, compound

https://huagongshe.com/reaction/323786

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22007146HCID 22007146—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 22007147HCID 2200714748.9%

Reaction Steps

A mixture of N-(m-Nitrobenzoyl)-4-methoxybenzenesulfonamide (920 mg, 2.87 mmol) and 100 mg of 10% Pd/C in ethanol (20 mL) was shaken under H2 (60 Psi) for 2 days at room temperature. After removing the catalyst by filtration, the filtrate was concentrated to afford 430 mg of the title compound which was used in the next reaction without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06214881B1
Source datasetuspto-grants-2001_04
ORD IDord-affcd92ba2fd4d62b467838e25c56f40
Source noteuspto-grants-2001_04