HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22007146, compound → HCID 22007147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22007146 | HCID 22007146 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22007147 | HCID 22007147 | 48.9% |
Reaction Steps
A mixture of N-(m-Nitrobenzoyl)-4-methoxybenzenesulfonamide (920 mg, 2.87 mmol) and 100 mg of 10% Pd/C in ethanol (20 mL) was shaken under H2 (60 Psi) for 2 days at room temperature. After removing the catalyst by filtration, the filtrate was concentrated to afford 430 mg of the title compound which was used in the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214881B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-affcd92ba2fd4d62b467838e25c56f40 |
| Source note | uspto-grants-2001_04 |