HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 88219091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 3-(2-Amino-1-hydroxyethyl)-4-methoxybenzene-1-sulfonamide | HCID 9906041 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 88219091 | HCID 88219091 | — |
Reaction Steps
Starting from (+)-α-aminomethyl-2-methoxy-5-sulphamoylbenzenemethanol treated with 1 equivalent of methanesulphonic acid in 2M solution in methanol, recrystallization in methanol and diethyl ether and drying in a desiccator under vacuum over phosphorus pentoxide, (+)-α-aminomethyl-2-methoxy-5-sulphamoylbenzenemethanol methanesulphonate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214882B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-e57b92a097924e2dbdb6a4c368df5158 |
| Source note | uspto-grants-2001_04 |