Phenethylamine → HCID 22007175, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:9]([S:12](=[O:15])(=[O:14])[NH2:13])=[CH:8][C:4]=1[CH:5]1[O:7][CH2:6]1.[CH2:16]([CH2:23][NH2:24])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[CH2:16]([CH2:23][NH:24][CH2:6][CH:5]([C:4]1[CH:8]=[C:9]([S:12](=[O:15])(=[O:14])[NH2:13])[CH:10]=[CH:11][C:3]=1[O:2][CH3:1])[OH:7])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1Participants
3
Procedure
2-Methoxy-5-sulphamoylstyrene oxide obtained in step 1 of Example 5, treated with benzylmethylamine under the conditions described in step 2 of Example 5, gives α-benzylmethylaminomethyl-2-methoxy-5-sulphamoylbenzenemethanol in the form of an oil.
Sources & evidence
- ORD record
- ord-8f9b50199cea447e83b787b502f8523e
- Source dataset
- uspto-grants-2001_04
- Patent number
- US06214882B1
Reaction notes
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