HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-diiodophenol → (1,1':3',1''-Terphenyl)-2'-ol, 5'-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-diiodophenol | HCID 10287922 | — |
| Reactant | N-(8-phenyl-octyl)-3,5-bis(m-trifluoromethylphenyl)4hydroxy-benzamide | HCID 22237600 | — |
| Product | (1,1':3',1''-Terphenyl)-2'-ol, 5'-phenyl- | HCID 3623729 | — |
Reaction Steps
The title compound was prepared as a solid (0.055 g, 28%, product 2: tris-arylation) from 4-bromo-2,6-diiodophenol using the procedure to step 2 of Example 40; 1H NMR (CDCl3) δ5.45 (s, 1H), 7.27-7.57 (m, 11H), 7.62 (d, J=8.3 Hz, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214877B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-4111e891bc844be3b6f1cee23bb66380 |
| Source note | uspto-grants-2001_04 |