HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15524306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15524305 | HCID 15524305 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15524306 | HCID 15524306 | — |
Reaction Steps
Methanol (20 ml) and 1N hydrochloric acid (2 ml) were added to the 4-(3-chloro-4-methoxybenzyl)amino-6-cyano-2-[3-(tetrahydropyran-2-yloxy)propyl]-1(2H)-phthalazinone (0.20 g) prepared in Example 24. The obtained mixture was stirred at room temperature for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218392B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-9dcacfdca6934eeaaa6d9e320ad64be5 |
| Source note | uspto-grants-2001_04 |