Benzo-1,3-dioxole-5-methylamine → HCID 21704216, compound

Participants

Reaction Steps

A mixture (4.83 g) comprising 1,6-dichloro-4-(3,4-methylenedioxybenzyl)aminophthalazine and 4,6-dichloro-1-(3,4-methylenedioxybenzyl)aminophthalazine was prepared from 1,4,6-trichlorophthalazine (3.38 g) prepared in Preparative Example 7 and piperonylamine (2.21 g) in a similar manner to that of Example 1. The title compound (0.22 g) was prepared from 0.8 g of the mixture in a similar manner to that of Example 3 as a less polar product.

Provenance & Evidence