HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 69307921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | HCID 69309629 | HCID 69309629 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 69307921 | HCID 69307921 | 76% |
Reaction Steps
Using alkylation method A, 3-chloro-N-[1-(4-fluoro-phenyl)-2-(piperidin-4-ylmethoxy)ethyl]-1H-indole-6-carboxamide (600 mg, 1.4 mmol) and acetone (10 mL, 135 mmol) afforded, after trituration (acetonitrile), 500 mg (76%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427632B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-d924d161d22940deac503ffab5e90c9d |
| Source note | uspto-grants-2008_09 |