Methyl 3-(bromomethyl)benzoate → (+/-)-3-[[5-(7-Ethyl-9,10-dihydro-2-methyl-4H-benzo[5,6]cyclohepta[1,2-d]oxazol-4-yl)-3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]methyl]benzoic acid, methyl ester

Participants

Role	Name	HCID	Charge
Reactant	Methyl 3-(bromomethyl)benzoate	HCID 517981	—
Reactant	(+/-)-5-(7-Ethyl-9,10-dihydro-2-methyl-4H-benzo[5,6]cyclohepta[1,2-d]oxazol-4-yl)-2,4(1H,3H)-pyrimidinedione	HCID 70114236	—
Product	(+/-)-3-[[5-(7-Ethyl-9,10-dihydro-2-methyl-4H-benzo[5,6]cyclohepta[1,2-d]oxazol-4-yl)-3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl]methyl]benzoic acid, methyl ester	HCID 131722510	—

Reaction Steps

The subtitle compound was prepared from the product of step (ii) (0.38 g) and methyl 3-[bromomethyl]benzoate according to the method of example 1 step (viii).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06218376B1
Source dataset	uspto-grants-2001_04
ORD ID	ord-d6c09d8b6e864a568deaf3bf7f670c5e
Source note	uspto-grants-2001_04