HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70114158, compound → HCID 70133637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70114158 | HCID 70114158 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70133637 | HCID 70133637 | — |
Reaction Steps
A solution of the product from step (ii) (0.44 g) in glacial acetic acid (10 ml) was stirred at room temperature overnight. The reaction mixture was evaporated to dryness (azeotroped twice with toluene) and the residue triturated with diethyl ether to give a pink solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218376B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-df4ab8303eb04a5c9bc815ebe838eeb7 |
| Source note | uspto-grants-2001_04 |