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HRID32445

反应详情

EQUATION

反应方程式

HRID 32445 的结构方程式

REACTANTS

反应物

2
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：Cl.O=C(N[C@@H](COCC1CCNCC1)c1ccccc1)OCc1ccccc1
HCID69308036

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)N1CCC(COC[C@H](NC(=O)OCc2ccccc2)c2ccccc2)CC1
HCID69307971

未命名化合物

PROCEDURE

实验过程

Using alkylation method A, benzyl N-[(R)-1-phenyl-2-(piperidin-4-ylmethoxy)ethyl]carbamate hydrochloride (3.7 g, 0.91 mmol) and acetone (2.3 g, 40 mmol) afforded, after purification (SiO2: 8:2:1 hexane:EtOAc:isopropylamine), 1.1 g (29%) of the title compound.

WORKUP

后处理

  1. customafforded
  2. customafter purification (SiO2: 8:2:1 hexane:EtOAc:isopropylamine), 1.1 g (29%) of the title compound