HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 69307971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | HCID 69308036 | HCID 69308036 | — |
| Product | HCID 69307971 | HCID 69307971 | — |
Reaction Steps
Using alkylation method A, benzyl N-[(R)-1-phenyl-2-(piperidin-4-ylmethoxy)ethyl]carbamate hydrochloride (3.7 g, 0.91 mmol) and acetone (2.3 g, 40 mmol) afforded, after purification (SiO2: 8:2:1 hexane:EtOAc:isopropylamine), 1.1 g (29%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427632B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-7969cd7c5a004d4c8fbde99400d76f86 |
| Source note | uspto-grants-2008_09 |