HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 178432307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 178432306 | HCID 178432306 | — |
| Product | HCID 178432307 | HCID 178432307 | — |
Reaction Steps
The title compound was prepared from the product of step (iii) (0.2 g) and Lawesson's reagent (0.9 g) according to the method of example 34 step (iv). Purification was by biotage chromatography on silica eluting with 5% methanol in dichloromethane with 1% 0.880 ammonia present to give a yellow glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218376B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-627cecf10c274e4dae8275e0e87f3d8c |
| Source note | uspto-grants-2001_04 |