HRID324482
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 40 °C
PROCEDURE
实验过程
A mixture of the product from step (i) (3.33 g), and 40% w/v aqueous methylamine solution was heated at 40° C. for 4 h. The solid was filtered and washed with water then dried under vacuum to give the subtitled product as a cream powder.
WORKUP
后处理
- filtrationThe solid was filtered
- washwashed with water
- customthen dried under vacuum