HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 22003631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 131722527 | HCID 131722527 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22003631 | HCID 22003631 | — |
Reaction Steps
The product from step (ii) (3.46 g) was treated with sodium hydroxide (0.7 g) in tetrahydrofuran (15 ml) and water (15 m) at room temperature. After 3 h the mixture was partitioned between 2M HCl and ethyl acetate. The organic phase was collected, dried (MgSO4) and solvent evaporated under reduced pressure to leave a colourless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218376B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-1fe122ffc1ad43009bd4d4e2c052f5d7 |
| Source note | uspto-grants-2001_04 |