HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 54563767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 22003631 | HCID 22003631 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54563767 | HCID 54563767 | — |
Reaction Steps
Oxalyl chloride (1.75 ml) was added to a solution of the product from step (iii) (3.14 g) in dichloromethane (30 ml) at room temperature containing 2 drops of dimethylformamide. After 4 h the volatiles were removed under reduced pressure to leave the subtitle product. Used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218376B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-704ed9495367406ebc74b36a35c6bbb5 |
| Source note | uspto-grants-2001_04 |