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HRID324498

反应详情

EQUATION

反应方程式

HRID 324498 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(P2(=S)SP(=S)(c3ccc(OC)cc3)S2)cc1
HCID87949

p-Anisyldithiophosphonic anhydride

C14H14O2P2S4

结构：Cn1cc(C2c3ccc(Cl)cc3C=Cc3sc(N4CCCC4)nc32)c(=O)[nH]c1=O
HCID70115681

未命名化合物

PRODUCTS

生成物

1
结构：Cn1cc(C2c3ccc(Cl)cc3C=Cc3sc(N4CCCC4)nc32)c(=S)[nH]c1=O
HCID88151786

未命名化合物

PROCEDURE

实验过程

The product from step (i) (0.04 g) was treated with Lawesson's reagent (0.037 g) according to the method of example 34 step (iv). Purification was by chromatography eluting with 1:1 ethyl acetate/isohexane to give the title product as a yellow solid.

WORKUP

后处理

  1. customPurification
  2. washeluting with 1:1 ethyl acetate/isohexane