HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Morpholinoethylamine → HCID 88151425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Reactant | (+/-)-5-(2,7-Dichloro-4H-benzo[5,6]cyclohepta[1,2-d]thiazol-4-yl)-1-methyl-2,4(1H,3H)-pyrimidinedione | HCID 70113243 | — |
| Product | HCID 88151425 | HCID 88151425 | — |
Reaction Steps
The subtitle product was prepared from the product of example 44 step (viii) (0.225 g) and 4-(2-aminoethyl)morpholine (0.38 ml) according to the method of example 51 step (i). Purification was by precipitation using diethyl ether with filtration to give the subtitle product as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218376B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-1d94a2d68210412eb844a7465158a732 |
| Source note | uspto-grants-2001_04 |