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HRID324500

反应详情

EQUATION

反应方程式

HRID 324500 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(P2(=S)SP(=S)(c3ccc(OC)cc3)S2)cc1
HCID87949

p-Anisyldithiophosphonic anhydride

C14H14O2P2S4

结构：Cn1cc(C2c3ccc(Cl)cc3C=Cc3sc(NCCN4CCOCC4)nc32)c(=O)[nH]c1=O
HCID88151425

未命名化合物

PRODUCTS

生成物

1
结构：Cn1cc(C2c3ccc(Cl)cc3C=Cc3sc(NCCN4CCOCC4)nc32)c(=S)[nH]c1=O
HCID88152166

未命名化合物

PROCEDURE

实验过程

The title product was prepared from the product of step (i) (0.162 g) and Lawesson's reagent (0.7 g) according to the method of example 34 step (iv). Purification was by chromatography eluting with dichloromethane/ethanol/triethylamine mixtures to give the title product as a yellow solid.

WORKUP

后处理

  1. customPurification
  2. washeluting with dichloromethane/ethanol/triethylamine mixtures