Lawesson's reagent → (+/-)-5-(7-Chloro-2-(2-(4-morpholinyl)ethylamino)-4H-benzo[5,6]cyclohepta[1,2-d]thiazol-4-yl)-1-methyl-3,4-dihydro-4-thioxo-2(1H)-pyrimidinone

Participants

Reaction Steps

The title product was prepared from the product of step (i) (0.162 g) and Lawesson's reagent (0.7 g) according to the method of example 34 step (iv). Purification was by chromatography eluting with dichloromethane/ethanol/triethylamine mixtures to give the title product as a yellow solid.

Provenance & Evidence