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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 324846Generated: October 30, 2026

HCID 67483831, compound → HCID 53697139, compound

https://huagongshe.com/reaction/324846

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67483831HCID 67483831—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 53697139HCID 53697139—

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.69-0.82 (m, 3 H), 1.09-1.40 (m, 14 H), 1.90 (m, 2 H), 3.20-3.45 (m, 2 H), 4.40 (m, 2 H), 5.25-5.45 (m, 1 H), 6.08 (m, 1H), 7.08-7.41 (m, 5 H). Rf=0.24 (10% ethyl acetate/n-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06218431B1
Source datasetuspto-grants-2001_04
ORD IDord-ef5fd5b41e3f43feb718686dc6ae0f13
Source noteuspto-grants-2001_04