HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67483831, compound → HCID 53697139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67483831 | HCID 67483831 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53697139 | HCID 53697139 | — |
Reaction Steps
The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.69-0.82 (m, 3 H), 1.09-1.40 (m, 14 H), 1.90 (m, 2 H), 3.20-3.45 (m, 2 H), 4.40 (m, 2 H), 5.25-5.45 (m, 1 H), 6.08 (m, 1H), 7.08-7.41 (m, 5 H). Rf=0.24 (10% ethyl acetate/n-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218431B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-ef5fd5b41e3f43feb718686dc6ae0f13 |
| Source note | uspto-grants-2001_04 |