HCID 67483578, compound → HCID 54380933, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.70 (t, J=7.5 Hz, 3 H), 1.10-1.40 (m, 15 H), 1.87 (tdd, J=7.5, 7.5, 1.5, 2 H), 1.95 (s, 3 H), 3.30-3.50 (m, 2 H), 4.20 (m, 1 H), 4.45 (m, 1 H), 5.30 (m, 1 H), 5.93 (m, 2 H), 6.90-7.30 (m, 4 H). FAB-MS: calculated for C24H33NO 352; found 352 (M+H, 100%). Rf=0.32 (10% ethyl acetate/n-hexane). mp 76-79° C.

Provenance & Evidence