HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67483535, compound → HCID 53963478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67483535 | HCID 67483535 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 53963478 | HCID 53963478 | — |
Reaction Steps
The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a 6:1 mixture of olefin isomers): δ 0.73-0.83 (m, 3 H), 1.10-1.40 (14 H), 1.91 (m, 2 H), 3.93 (m, 2 H), 4.39 (d, J=5.0 Hz, 2 H), 5.25-5.45 (m, 1 H), 5.98 (m, 1 H), 7.11 (m, 2 H), 7.35 (m, 2 H). Rf=0.36 (10% ethyl acetate/n-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218431B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-ec2e823c12f24e2e82d80d2a18359b6f |
| Source note | uspto-grants-2001_04 |