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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 324852Generated: October 30, 2026

HCID 67483535, compound → HCID 53963478, compound

https://huagongshe.com/reaction/324852

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67483535HCID 67483535—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 53963478HCID 53963478—

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a 6:1 mixture of olefin isomers): δ 0.73-0.83 (m, 3 H), 1.10-1.40 (14 H), 1.91 (m, 2 H), 3.93 (m, 2 H), 4.39 (d, J=5.0 Hz, 2 H), 5.25-5.45 (m, 1 H), 5.98 (m, 1 H), 7.11 (m, 2 H), 7.35 (m, 2 H). Rf=0.36 (10% ethyl acetate/n-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06218431B1
Source datasetuspto-grants-2001_04
ORD IDord-ec2e823c12f24e2e82d80d2a18359b6f
Source noteuspto-grants-2001_04