HCID 54469891, compound → HCID 22005166, compound

Participants

Reaction Steps

The title compound was prepared from 2,6-diisopropyl-3-hydroxymethyl-4-(3-chlorophenyl)-5-(pent-1-enyl)pyridine (Example 145) by the procedure described in Example 126. 1H NMR (300 MHz, CDCl3): δ 0.80 (t, J=7.0 Hz, 3 H), 1.0-1.40 (m, 19 H), 2.26 (m, 2 H), 3.23 (m, 1 H) 3.41 (m, 1 H), 4.34 (m, 2 H), 7.05-7.45 (m, 4 H). FAB-MS: calculated for C23H32NOCl 374; found 374 (M+H, 100%). Rf0.26 (10% ethyl acetate/n-hexane). mp 94-95° C.

Provenance & Evidence