HCID 67483358, compound → HCID 54517473, compound

HRID 324856Notes

Reaction equation

HRID 324856 reaction equation
[CH:1]([C:4]1[C:9]([C:10](OCC)=[O:11])=[C:8]([C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=2[Cl:22])[C:7]([CH:23]=[CH:24][CH2:25][CH2:26][CH3:27])=[C:6]([CH:28]([CH3:30])[CH3:29])[N:5]=1)([CH3:3])[CH3:2]>C(OCC)(=O)C.CCCCCC>[CH:1]([C:4]1[C:9]([CH2:10][OH:11])=[C:8]([C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=2[Cl:22])[C:7]([CH:23]=[CH:24][CH2:25][CH2:26][CH3:27])=[C:6]([CH:28]([CH3:29])[CH3:30])[N:5]=1)([CH3:3])[CH3:2]

Participants

3

Reactant 1

HCID 67483358HCID 67483358, compound

Product 1

HCID 54517473HCID 54517473, compound

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a 1:1 mixture of olefins): δ 0.75-0.87 (m, 3 H), 1.13-1.37 (m, 14 H), 1.65-2.0 (m, 2 H), 3.20-3.51 (m, 2 H), 4.30 (m, 1 H), 4.42 (m, 1 H), 5.31-5.50 (m, 1 H), 6.0 (m, 1 H), 7.05 (m, 1 H), 7.28 (m, 1 H), 7.47 (m, 1 H). Rf0.38 (10% ethyl acetate/n-hexane).

Sources & evidence

ORD record
ord-2f28f8a078804386b1d83343d3ddee91
Source dataset
uspto-grants-2001_04
Patent number
US06218431B1

Reaction notes

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