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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 324856Generated: October 31, 2026

HCID 67483358, compound → HCID 54517473, compound

https://huagongshe.com/reaction/324856

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67483358HCID 67483358—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 54517473HCID 54517473—

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a 1:1 mixture of olefins): δ 0.75-0.87 (m, 3 H), 1.13-1.37 (m, 14 H), 1.65-2.0 (m, 2 H), 3.20-3.51 (m, 2 H), 4.30 (m, 1 H), 4.42 (m, 1 H), 5.31-5.50 (m, 1 H), 6.0 (m, 1 H), 7.05 (m, 1 H), 7.28 (m, 1 H), 7.47 (m, 1 H). Rf0.38 (10% ethyl acetate/n-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06218431B1
Source datasetuspto-grants-2001_04
ORD IDord-2f28f8a078804386b1d83343d3ddee91
Source noteuspto-grants-2001_04