HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67483358, compound → HCID 54517473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67483358 | HCID 67483358 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 54517473 | HCID 54517473 | — |
Reaction Steps
The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a 1:1 mixture of olefins): δ 0.75-0.87 (m, 3 H), 1.13-1.37 (m, 14 H), 1.65-2.0 (m, 2 H), 3.20-3.51 (m, 2 H), 4.30 (m, 1 H), 4.42 (m, 1 H), 5.31-5.50 (m, 1 H), 6.0 (m, 1 H), 7.05 (m, 1 H), 7.28 (m, 1 H), 7.47 (m, 1 H). Rf0.38 (10% ethyl acetate/n-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06218431B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-2f28f8a078804386b1d83343d3ddee91 |
| Source note | uspto-grants-2001_04 |