HCID 67483422, compound → HCID 54345918, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step A by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.74 (t, J=7.4 Hz, 3 H), 1.25 (m, 14 H), 1.90 (m, 2 H), 3.39 (m, 2 H), 4.39 (d, J=6.0 Hz, 2 H), 5.07 (s, 2 H), 5.32 (m, 1 H), 5.97 (m, 1 H), 6.74 (m, 2 H), 6.95 (m, 1 H), 7.35 (m, 7 H). FAB-MS: calculated for C30H37NO2, 444; found 444 (M+H, 100%). Elemental analysis: calculated for C30H37NO2: C 81.22; H 8.41; N 3.16, found: C 80.51; H 8.41; N 3.36. Rf 0.5 (25% ethyl acetate/n-hexane).

Provenance & Evidence