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HRID324860

反应详情

EQUATION

反应方程式

HRID 324860 的结构方程式

REACTANTS

反应物

3
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：CCOC(=O)CC(=O)C(C)C
HCID81583

Ethyl isobutyrylacetate

C8H14O3

结构：O=Cc1ccccc1I
HCID643439

Benzaldehyde, 2-iodo-

C7H5IO

PRODUCTS

生成物

1
结构：CCOC(=O)c1c(C(C)C)nc(C(C)C)c(C(=O)OCC)c1-c1ccccc1I
HCID22005000

未命名化合物

PROCEDURE

实验过程

Prepared from 2-iodobenzaldehyde, ethyl isobutyrylacetate and concentrated ammonium hydroxide by the procedures described in Example 125, Steps A-B. 1H NMR (300 MHz, CDCl3): δ 0.94 (t, J=7.0 Hz, 6 H), 1.30 (d, J=6.6 Hz, 6 H), 1.34 (d, J=6.6 Hz, 6 H), 3.19 (septet, J=6.6 Hz, 2 H), 4.0 (q, J=7.0 Hz, 4 H), 7.0-7.40 (m, 3 H), 7.85 (m, 1 H).