HCID 86756634, compound → HCID 73858735, compound

Participants

Reaction Steps

The title compound was prepared from the intermediate obtained in Step D by the procedure described in Example 125, Step F. 1H NMR (300 MHz, CDCl3) (reported as a mixture of olefin isomers): δ 0.81 (t, J=7.4 Hz, 3 H), 1.0-1.40 (m, 15 H), 1.75 (m, 2 H), 2.98 (d, J=3.3 Hz, 1 H), 3.20-3.60 (m, 2 H), 4.20-4.50 (m, 2 H), 5.40 (m, 1 H), 6.0 (m, 1 H), 7.0-7.60 (m, 4 H). Rf=0.23 (10% ethyl acetate/n-hexane).

Provenance & Evidence