Ammonia → n-Octadecenyl-succinic monoamide

HRID 324907Notes

Reaction equation

HRID 324907 reaction equation
[NH3:1].[CH:2]([CH:20]1[CH2:25][C:24](=[O:26])[O:23][C:21]1=[O:22])=[CH:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].Cl>C(#N)C>[CH:2]([CH:20]([CH2:25][C:24]([OH:23])=[O:26])[C:21]([NH2:1])=[O:22])=[CH:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

5

Reactant 3

HCID 222AmmoniaHCID 313Hydrochloric AcidHCID 225771Dihydro-3-(1-octadecen-1-yl)-2,5-furandione

Product 1

HCID 86756637n-Octadecenyl-succinic monoamide

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

389 g of a 25% aqueous ammonia was mixed with 200 ml of acetonitrile and to the mixture was added 100 g of n-octadecenylsuccinic anhydride, followed by stirring for 2 hours at room temperature. The mixture was neutralized with concentrated hydrochloric acid. The crystals thus-deposited were collected by filtration, washed with water and then with acetonitrile, and dried to obtain 84.5 g of n-octadecenyl-succinic monoamide as colorless crystals.

Workup

  1. filtrationThe crystals thus-deposited were collected by filtration
  2. washwashed with water
  3. dry with materialwith acetonitrile, and dried

Sources & evidence

ORD record
ord-373662ac0fcd4d7cba87f7d6ad92f2e5
Source dataset
uspto-grants-2001_04
Patent number
US06220925B1

Reaction notes

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