HRID324907

反应详情

EQUATION

反应方程式

HRID 324907 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

389 g of a 25% aqueous ammonia was mixed with 200 ml of acetonitrile and to the mixture was added 100 g of n-octadecenylsuccinic anhydride, followed by stirring for 2 hours at room temperature. The mixture was neutralized with concentrated hydrochloric acid. The crystals thus-deposited were collected by filtration, washed with water and then with acetonitrile, and dried to obtain 84.5 g of n-octadecenyl-succinic monoamide as colorless crystals.

WORKUP

后处理

  1. filtrationThe crystals thus-deposited were collected by filtration
  2. washwashed with water
  3. dry with materialwith acetonitrile, and dried