HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyacetic Acid → Phenoxyacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyacetic Acid | HCID 19188 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Phenoxyacetyl chloride | HCID 69703 | — |
Reaction Steps
Phenoxyacetic acid (d5) was treated with 25 ml of thionyl chloride and stirred for 18 hours at room temperature. After the 5 end of the reaction, the reaction mixture was concentrated under vacuum at 300 C to provide phenoxyacetyl chloride (4.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06221335B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-8715d0b84f814f46a2b1c5e81a732046 |
| Source note | uspto-grants-2001_04 |