HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 325131Generated: October 31, 2026
HCID 11459419, compound → HCID 18371077, compound
https://huagongshe.com/reaction/325131
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 11459419 | HCID 11459419 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 18371077 | HCID 18371077 | — |
Reaction Steps
A mixture of 25.2 g 3-oxo-5-(2,6,6-trimethyl-cyclohex-2-enyl)-pentanoic acid methyl ester and 4.3 g ethylene glycol was slowly heated to 180° C. while distilling off methanol. On completion, the reaction mixture was chromatographed over silica gel to yield a colourless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06222062B1 |
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| Source dataset | uspto-grants-2001_04 |
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| ORD ID | ord-727795adb21c4862b3feb333b7425f83 |
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| Source note | uspto-grants-2001_04 |
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