Styrene → HCID 3807119, compound

HRID 325138Notes

Reaction equation

HRID 325138 reaction equation
[CH3:1][NH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH2:9]=[CH:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>C(OCC)(=O)C.CCCCCC>[CH3:1][N:2]([CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 7501StyreneHCID 7515N-Methylaniline

Product 1

HCID 3807119HCID 3807119, compoundYield 53%

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

According to GWM, 0.011 mol (=1.20 ml) of N-methylaniline and 0.011 mol (=1.00 ml) of styrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:3) as eluent, the product N-methyl-N-phenylethylaniline being obtained as a yellow liquid.

Workup

  1. customare reacted with one another
  2. customThe product is isolated by column chromatography

Sources & evidence

ORD record
ord-a59e2833f8f3486d80754c5e95005b6a
Source dataset
uspto-grants-2001_04
Patent number
US06222073B1

Reaction notes

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