HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20465224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 20465207 | HCID 20465207 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20465224 | HCID 20465224 | — |
Reaction Steps
2-Mercapto-3-trifluoromethyl-benzoic acid (4.0 g, 18 mmol), acetic anhydride (2.2 g, 22 mmol), and glacial acetic acid (6 ml) were refluxed 30 minutes, cooled and combined with dilute hydrochloric acid, thereby affording the product as a white crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04440941 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-22e8deaf4edc491a89c1fd69fc6c8ad7 |
| Source note | uspto-grants-1984_04 |