Hydrochloric Acid → HCID 20465224, compound

HRID 325486Notes

Reaction equation

HRID 325486 reaction equation
[SH:1][C:2]1[C:10]([C:11]([F:14])([F:13])[F:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[C:15](OC(=O)C)(=[O:17])[CH3:16].Cl>C(O)(=O)C>[C:15]([S:1][C:2]1[C:10]([C:11]([F:12])([F:13])[F:14])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])(=[O:17])[CH3:16]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 7918Acetic AnhydrideHCID 20465207HCID 20465207, compound

Product 1

HCID 20465224HCID 20465224, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

2-Mercapto-3-trifluoromethyl-benzoic acid (4.0 g, 18 mmol), acetic anhydride (2.2 g, 22 mmol), and glacial acetic acid (6 ml) were refluxed 30 minutes, cooled and combined with dilute hydrochloric acid, thereby affording the product as a white crystalline solid.

Workup

  1. temperaturecooled

Sources & evidence

ORD record
ord-22e8deaf4edc491a89c1fd69fc6c8ad7
Source dataset
uspto-grants-1984_04
Patent number
US04440941

Reaction notes

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