HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Acetylthio-3-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-Mercapto-3-methoxybenzoic acid | HCID 16655610 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Acetylthio-3-methoxybenzoic acid | HCID 20465211 | — |
Reaction Steps
A solution of 2-mercapto-3-methoxybenzoic acid (14.6 g, 79 mmol), acetic anhydride (9.7 g, 95 mmol) and glacial acetic acid (35 ml) was refluxed 15 minutes, then cooled and poured into dilute hydrochloric acid. The product was vacuum-filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04440941 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-30eff028606941938fb119fa7a2bed0d |
| Source note | uspto-grants-1984_04 |