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HRID325498

反应详情

EQUATION

反应方程式

HRID 325498 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：COc1cccc(C(=O)O)c1S
HCID16655610

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(C(=O)O)c1SC(C)=O
HCID20465211

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A solution of 2-mercapto-3-methoxybenzoic acid (14.6 g, 79 mmol), acetic anhydride (9.7 g, 95 mmol) and glacial acetic acid (35 ml) was refluxed 15 minutes, then cooled and poured into dilute hydrochloric acid. The product was vacuum-filtered.

WORKUP

后处理

  1. temperaturecooled
  2. filtrationThe product was vacuum-filtered